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Your Position: Home > DOCUMENTS & REFERENCE > CERTIFICATE OF ANALYSIS > (S,S,S)-2-Azabicyclo[3,3,0]octane-3-carboxylic Acid Benzyl E

(S,S,S)-2-Azabicyclo[3,3,0]octane-3-carboxylic Acid Benzyl E

Certification of Analysis

 

Product Name

(S,S,S)-2-Azabicyclo[3,3,0]octane-3-carboxylic Acid Benzyl Ester Hydrochloride

Catalog No

SC-07384

CAS Number

93779-31-8

Quantity    

100g

Batch No

20101010

Product Date 

2010.1.10

Date of analysis  

2010.10.10

 

 

 

 

 

 

 

 

 

 

Items of analysis

Specification

Results

Appearance

Off-white to light brown colored powder

White crystalline powder

IdentificationHPLC

Retention time of RMP- peak in the sample preparation should be concordant with that of standard preparation

Conforms

Melting range

172.0~184.0

180.5

Specific rotation

-35.0°~-41.0°

-39.0°

Loss on drying

1.0%

0.11%

Residue on ignition

0.2%

0.08%

Related substances

RRT0.53 impurity: not more than 0.3%

Not detectable

RRT0.83 impurity: not more than 0.3%

Not detectable

Single maximum impurity: not more than 0.15%

0.04%

Total impurities: not more than 1.0%

0.1%

Assay(by titration)

98.0%102.0%

100.4%

Conclusion

It accords with the Enterprise Standard

       

 

 

Analyst:  Carlos Lin                                              Check: Sally Chen                                                           Date:    2010-10-10